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| Industry | : Chemical | | Product | : Inductive conductivity meters |
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Measurement of Concentration of Supersaturated NaCl Solution in Salt Dissolvers at Electrolysis Plants
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Control of sodium chloride (NaCl) concentration at a salt
dissolver where solid salt is dissolved in water, is highly
important because of the electrolysis efficiency. A conventional
way of measuring the concentration of supersaturated NaCl
solution had been performed by using non-contact type sensors
(e.g., γ-ray density meter) since NaCl, impurities, and precipitates
are in the solution. In this way, there were disadvantages such
as troublesome maintenance and therefore, the radiation control
is required for γ-ray density meter.
Responding to these backgrounds, the ISC202 inductive
conductivity meter provides concentration reading and realizes
to improve substantial maintainability, cost performance and
measurement accuracy.
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Measures NaCl concentration in salt dissolvers |
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Reduces operating costs |
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In an electrolysis plant, the solid salt is dissolved in water in a salt dissolver to make brine. This brine contains impurities, such
as calcium, magnesium or sulfates, that decrease electrolysis efficiency. The brine is purified by removing these impurities before
being fed to an electrolyzer, where the purified brine is electrolyzed to produce caustic soda and chlorine. The caustic soda solution
produced at the cathode in the electrolyzer is concentrated in a multiple effect evaporator, as a result the concentration is increased from
approximately 32% to 48%. |
| Measurement system |
| 2-wire inductive conductivity system |
| Sensor |
ISC40G(J)-GG-T1-☐☐ |
| Flow-through holder |
ISC40FF(J)-PJ |
| Transmitter |
ISC202G-1-E/SPS
(with screws for salt protection) |
| Dedicated distributor for transmitter |
PH201G-A☐*B |
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Inductive Conductivity Sensor & Transmitter Installation Diagram
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| ISC202G inductive conductivity transmitter |
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Power supply voltage: |
17 - 40 V DC (from distributor) |
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Power consumption: |
0.9 VA maximum |
| PH201G distributor |
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Power supply: 100 V: |
20 to130 V DC/80 to 138 V AC, 47 to 63 Hz |
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220 V: |
120 to 340 V DC/138 to 264 V AC, 47 to 63 Hz |
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Power consumption: |
24 V DC: approx. 200 mA |
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100 V AC: approx. 7 VA |
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220 V AC: approx. 11 VA |
Notes
Sampling should be done in the supernatant liquid in a salt dissolver.
The supernatant liquid is collected in a settling tank and then the
supernatant liquid of the tank is transported to a measurement tank
where the sensor is installed.
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| 1. Process conditions (salt dissolver) |
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Temperature: |
Approx. 65°C |
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Pressure: |
Atmospheric pressure |
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Sample: |
Supersaturated brine |
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NaCl concentration control range: 200 to 360 g/L |
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--> 18.1 to 30 wt%* |
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* Depends on user's actual data of specific gravity. |
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| 2. ISC202G setting parameters |
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Relationship between conductivity and concentration is based
on the linear approximation of
S = 16.3x that is obtained by actual measurement using SC72
Personal Conductivity Meter. |
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NaCl temperature compensation table is used |
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Reference temperature setting: 25°C |
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Output setting: Code 04 |
| Output (%) |
Concentration (%) |
Conductivity (mS/cm) |
| 0 |
18 |
293 |
| 50 |
24 |
391 |
| 100 |
30 |
489 |
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Measurement of Supersaturated NaCl Concentration |
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